Fig. 3

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(a) X-ray diffractograms (20° ≤ 2θ ≤ 65°) recorded at different temperatures during in situ annealing of a Mg/Sb bilayer (stars for Mg3Sb2 and diamonds for Sb), (b) normalized intensities of the Mg3Sb2(002) and Sb(012) peaks as a function of temperature.

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