Table 1
TEM characteristic parameters obtained on as-prepared and annealed samples with low density (LD) and high density (HD) for monomer diameter (D1) and deviation (σ1) from Gaussian fit of size histogram, for mean size (Dmean) in the spherical approximation; for mean distances edge to edge between nearest neighbors (NN) and for density nanoparticles per area (ρ) from imageJ analysis.
| Sample | D1 (n/m) | σ1 (n/m) | Dmean (n/m) | NN (n/m) | ρ (NPs/μ2) | |
|---|---|---|---|---|---|---|
| LD | as prepared | 7.6 | 0.5 | 8.7 | 6.4 | 1362 |
| annealed | 6.3 | 0.4 | 6.9 | 9.8 | 1236 | |
| HD | as prepared | 7.2 | 0.7 | 10.4 | 2.9 | 2195 |
| annealed | 6.5 | 0.6 | 8.9 | 5.0 | 2600 |
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