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Cited article:

Magnetic Iron Oxide Nanoparticles in 10−40 nm Range: Composition in Terms of Magnetite/Maghemite Ratio and Effect on the Magnetic Properties

Jaime Santoyo Salazar, Lucas Perez, Oscar de Abril, et al.
Chemistry of Materials 23 (6) 1379 (2011)
https://doi.org/10.1021/cm103188a